REW file:
The data looks valid, but I'm not really sure what I'm looking at there! Is that just one of the speakers by itself, or both together? Was that measured at the mix position, in the middle of where your head will be?
I hope I am doing it right. I'm not sure the SPL calibration is quite right - the REW SPL and my SPL do not match even after telling it that I'm reading 75dBC.
I don't understand: If you calibrated REW at a certain level, then it should always remain calibrated to that level... unless you changed something! Are you certain that you had only ONE speaker running when you did that calibration? You must do each one individually (with the other one turned off), not both together. And use a level of 80 dBC, with the full-range main speaker pink-noise test signal in REW. Make sure you are not using the sub-woofer calibration signal by accident. (Even though the REW manual says to use 75, actually 80 is correct.)
So you get REW to play out the pink noise tone at -12dB on the REW "preferences" meter, and you make sure that it is going through your complete signal chain at 0 dBu (-20 dbFS for the digital parts of your system), and that signal is getting to just ONE speaker. Then you adjust your speaker volume control for that speaker alone, until you see a level of 85 dBC on your hand-held sound level meter. At that point, you hit the "SPL Meter" button on REW, set it to "SPL", "C" and "S", hit the "Calibrate" button, select "REW Speaker cal signal", and you should then hear the same pink-noise signal as before coming from ONLY the speaker that you are calibrating, and it should still show up as 80 dBC on your hand held meter. You then type the exact number that you are seeing on your hand-held meter, into the "SPL Reading Calibration" box, and hit "finished". Now repeat the same process for the OTHER speaker, all by itself. As a final check, turn on BOTH speakers, send the calibration signal to BOTH speakers, and check that the level is 86 dBC. Don't re-calibrate here! Just check.
That's it! If you do that correctly, then there is no reason why it would the levels would not match in the future. They would only fail to match if you adjsuted something in the signal chain, such as the volume control on the speaker, or the gain control on your console, or the fader position, or the mic. As long as you don't touch any of that, then the sound level in the room and the sound level shown by both your hand-held meter and the REW meter, will all be the same.
I should say, it already impresses me no end how I can see cars but not hear them!
Aren't you glad you came to the forum, and found what you needed here to do that?
So we can say that your isolation goal is achieved?
I've covered all fibreglass for now with plastic ...

Ummmm.... that's not the way to do it.... I'll get into that below. Think of it like this: When you take a shower, do you first put on your raincoat, plastic cap, gloves, and goggles?
For some reason I was obsessing about getting the right plastic,
Pity you didn't listen to your obsession! It was right....

(more on that later...)
in the end I just got some drop sheets from the hardware store and at least they contain the fibres
Right result, wrong method. . .
- some slats (they also look cool so i hope I need them!)
You probably do, but a slat resonators wont' work any more in your room, because you covered the "resonator" part with plastic!

A slot resonator is a tuned device. There's a "slug" of air trapped between the slats, that moves in and out in sympathetic resonance with certain frequencies. What governs that frequency, is the mass of the air that is trapped in there, and the depth of the air cavity behind the slats (from the back of the slat to the surface of the wall behind it). As the slug of air moves in and out, it compresses and expands the air trapped in the cavity, causing it to act like a spring. So you have the
mass of the slug of air, and the
spring in the cavity behind it. Mass+spring = resonant system. It really, really wants to vibrate a certain frequency. And because you have insulation inside the cavity, that puts a massive damper on the vibrations. So whenever that specific frequency comes along, the things tries to resonate, but can't do that very well, since the insulation damps it, and absorbs the energy. And that's good! It takes energy out of the room at that frequency. So each slot in your slot wall will absorb a certain frequency (or range of frequencies).
Or rather it would have if you built it correctly, but seeing that you put plastic over everything, there is no air connection between the air slug and the spring, thus no resonance, and no absorption....
In other words; because you plastered the entire room with plastic, you now cannot have slot walls. Out of the question. They won't work, even though you do need them. . .
One big concern I have, is that I have noticed a bit of tinnitus when sitting in the room and also when in my bed morning and night.
Probably not entirely due to the room, unless you have been listening at levels that are to high, but maybe partially due to that. More on that later . . .
Or whether having fully plastic wrap is hitting my ears with a high frequency refelction & doing me no good.

Bingo!
I had a go at getting REW going, for interest as much as anything
This is your first measurement, with the empty room. It is your baseline, against which all future measurements will be compared, to see how you are progressing. So far from being "just for interest", this is actually the single most important test you will do! It should be done with the greatest of care, to ensure that it is absolutely valid, and totally accurate.
But anyway: what does it say?
First, the obvious part. Low end waterfall plot:
NickLear-empty-baseline-WF-17..500.jpg
You clearly don't have any bass trapping in the room! You have very obviously visible modal ringing at 41 Hz, 82 Hz and 123 Hz. In the image above, I'm highlithing your 82Hz mode, as it is pretty big! There's also tiny signs of activity at 164 Hz, and 205 Hz.... Notice the relationship?

That's your 1.0.0, 2.0.0, and 3.0.0 modes. In other words, the axial modes related to the length of the room. (Which you said was 4.02 m long). There's also small sings of stuff at 62 Hz and 67 Hz, which would be your 0.1.0 and 0.0.1 modes. There's even signs of tangential and oblique modes. (So much for those silly simple calculators that ignore such modes, claiming they are "not important....").
So, clearly, your next step is getting the bass traps in. Big ones. Deep ones. Large ones. Front and back walls, for sure.
I only did it from 30Hz to protect my speakers,
Protect them from what? From producing sound waves? Isn't that what they are supposed to do?

That's like putting plastic covers on your car tyres, to protect them from the road...

Since you did not run full-spectrum tests, we can't see what is going on in the very low end of your room. Hopefully, nothing, since your lowest mode is 41 Hz, but there might also be other stuff happening, such as "chuffing" in your speaker reflex ports, or resonances in the room structure...
Now for the sad part:
NickLear-empty-baseline-RT-40..12k.jpg
That's your decay time curve, for the enter spectrum. For usable acoustics, it should look like this:
RMOUS-14-J-29-RT30.png
Flat. That's what you want. The decay times must be the same across the entire spectrum: in other words, all frequencies in the room must die away at the exact same rate, and that rate must be the correct rate for your room: around 170 ms, give or take a bit. Yours is currently around 250 ms, total, but it varies wildly from as little as 60 ms in the mid range to around 280 ms in the high end (can you say "overdone plastic"?), and 350 in the low end! You can see that clearly in the full-spectrum waterfall-plot:
NickLear-empty-baseline-WF-20..14k.jpg
Why is that? Well, it's because you don't have any bass trapping in the low end, you are over-absorbing the mid range, and massively boosting the high end around the entire room because you covered the whole darn thing with thin plastic!!!!
The entire room is now reflective at high frequencies, absorptive at mid frequencies, and resonant in low frequencies.
I have noticed a bit of tinnitus when sitting in the room ...
Yup!
- Stuart -